HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propanal → HCID 86658990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propanal | HCID 527 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | HCID 10943005 | HCID 10943005 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 86658990 | HCID 86658990 | — |
Reaction Steps
The title compound was prepared from (E)-(4-nitrobut-3-enyl)benzene and propionaldehyde according to general procedure. The enantiomeric excess was determined by HPLC with Chiralpak AD-H column at 210 nm (2-propanol:hexane=2:98), 1 mL/min, tmajor=15.4 min, tminor=14.4 min, the diastereomeric ratio was determined by
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206090B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-2c52091274254c79b309b1121fbc3531 |
| Source note | uspto-grants-2015_12 |