HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 58500186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 3-Methylbutanal | HCID 11552 | — |
| Reactant | 37630-26-5 | HCID 5381679 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 58500186 | HCID 58500186 | — |
Reaction Steps
The title compound was prepared from (E)-1-(2-nitrovinyl)naphthalene and isovaleraldehyde according to general procedure. The enantiomeric excess was determined by HPLC with Chiralpak AD-H column at 254 nm (2-propanol:hexane=10:90), 1 mL/min, tmajor=13.7 min, tminor 16.8 min, the diastereomeric ratio was determined by
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206090B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-e96e64b1b10f4758aa61d7efa365fb13 |
| Source note | uspto-grants-2015_12 |