HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 54588982, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | 3-Fluoro-4-morpholinobenzoic acid | HCID 12109595 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54588982 | HCID 54588982 | — |
Reaction Steps
This compound may be prepared from (14) in a one pot reaction utilizing POCl3 in DMF (Vilsmeier complex) and NaN3 following the literature procedure of Sridhar et al. (Syn. Comm. 2003, 33, 607-611).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206141B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-9ec38df0238b438fb578f2d1c4caba17 |
| Source note | uspto-grants-2015_12 |