HCID 73603447, compound → HCID 73603448, compound

Participants

Reaction Steps

The product of Step 6 of Example 8 and the product of Step 1 of Example 15 are reacted using the same procedure as step 6—Example 8 and making non-critical variations the title compound is obtained (358 mg): 1H NMR (DMSO-d6) 4.27 (2H, s), 4.47-4.32 (2H, m), 4.70-4.56 (1H, m), 4.91 (1H, s), 5.92 (1H, d), 6.23 (1H, t), 7.50 (3H, m), 7.74 (2H, d), 8.15 (1H, d), 8.84 (1H, d), 8.91 (1H, s); m/z 363.1 (M+H)+.

Provenance & Evidence