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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1500405Generated: November 1, 2026

Ethyl chloroacetate → HCID 131734275, compound

https://huagongshe.com/reaction/1500405

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthyl chloroacetateHCID 7751—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 178419808HCID 178419808—
SolventAcetoneHCID 180—
ProductHCID 131734275HCID 131734275—

Reaction Steps

A mixture of 5-(1,3-benzodioxol-5-yl)-1H-tetrazole (10 mmol), ethyl chloroacetate (10 mmol) and potassium carbonate (15 mmol) in dry acetone (100 mL) was refluxed for 24 h. The reaction mixture was filtered, the solvent was distilled. The crude ester thus obtained was purified by recrystallization from ethanol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09206165B2
Source datasetuspto-grants-2015_12
ORD IDord-60c1001a8d184328a9a4e89392fcf842
Source noteuspto-grants-2015_12