HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroacetate → HCID 131734275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroacetate | HCID 7751 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178419808 | HCID 178419808 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 131734275 | HCID 131734275 | — |
Reaction Steps
A mixture of 5-(1,3-benzodioxol-5-yl)-1H-tetrazole (10 mmol), ethyl chloroacetate (10 mmol) and potassium carbonate (15 mmol) in dry acetone (100 mL) was refluxed for 24 h. The reaction mixture was filtered, the solvent was distilled. The crude ester thus obtained was purified by recrystallization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206165B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-60c1001a8d184328a9a4e89392fcf842 |
| Source note | uspto-grants-2015_12 |