HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86718008, compound → HCID 86718009, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86718008 | HCID 86718008 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86718009 | HCID 86718009 | — |
Reaction Steps
The mixture of (R)-2,5-dimethyl-7-nitro-2,3-dihydrobenzofuran (3e) (0.84 g, 4.3 mmol) and Pd/C (100 mg, 15%) in THF (10 mL) was introduced H2 at ambient temperature. It was stirred at ambient temperature for 12 h. The mixture was filtered through Celite and concentrated to give the title compound (3f) as a solid. MS-ESI (m/z): 164 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206166B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-a1152d0534f648f7977fa159ea8673db |
| Source note | uspto-grants-2015_12 |