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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1500471Generated: November 3, 2026

HCID 86718008, compound → HCID 86718009, compound

https://huagongshe.com/reaction/1500471

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86718008HCID 86718008—
CatalystPalladiumHCID 23938—
SolventTetrahydrofuranHCID 8028—
ProductHCID 86718009HCID 86718009—

Reaction Steps

The mixture of (R)-2,5-dimethyl-7-nitro-2,3-dihydrobenzofuran (3e) (0.84 g, 4.3 mmol) and Pd/C (100 mg, 15%) in THF (10 mL) was introduced H2 at ambient temperature. It was stirred at ambient temperature for 12 h. The mixture was filtered through Celite and concentrated to give the title compound (3f) as a solid. MS-ESI (m/z): 164 (M+1)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09206166B2
Source datasetuspto-grants-2015_12
ORD IDord-a1152d0534f648f7977fa159ea8673db
Source noteuspto-grants-2015_12