HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86718027, compound → HCID 86718028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86718027 | HCID 86718027 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86718028 | HCID 86718028 | — |
Reaction Steps
A mixture of 2-(methoxymethyl)-5-methyl-7-nitro-2,3-dihydrobenzofuran (8a) (0.85 g, 3.8 mmol) and Pd/C (90 mg, 10%) in THF (10 mL) was introduced H2 and stirred at ambient temperature for 12 h. The mixture was filtered through celite and concentrated to give the title compound (8b) as oil. MS-ESI (m/z): 194 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206166B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-8bc299d048cc49e8a9187d5c68f33c11 |
| Source note | uspto-grants-2015_12 |