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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1500490Generated: October 31, 2026

HCID 86718027, compound → HCID 86718028, compound

https://huagongshe.com/reaction/1500490

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86718027HCID 86718027—
CatalystPalladiumHCID 23938—
SolventTetrahydrofuranHCID 8028—
ProductHCID 86718028HCID 86718028—

Reaction Steps

A mixture of 2-(methoxymethyl)-5-methyl-7-nitro-2,3-dihydrobenzofuran (8a) (0.85 g, 3.8 mmol) and Pd/C (90 mg, 10%) in THF (10 mL) was introduced H2 and stirred at ambient temperature for 12 h. The mixture was filtered through celite and concentrated to give the title compound (8b) as oil. MS-ESI (m/z): 194 (M+1)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09206166B2
Source datasetuspto-grants-2015_12
ORD IDord-8bc299d048cc49e8a9187d5c68f33c11
Source noteuspto-grants-2015_12