Hydrochloric Acid → HCID 117778124, compound

Participants

Reaction Steps

To tert-butyl N-tert-butoxycarbonyl-N-[(3-cyclopentylphenyl)methyl]carbamate (4.70 g), a solution of hydrogen chloride in ethyl acetate (4 M, 50 mL) was added, and the mixture was then stirred at room temperature for 2 hours. The reaction solution was concentrated under reduced pressure, and ether (200 mL) was added to the residue. The resulting suspension was filtered, and the product collected by filtration was dried under reduced pressure to obtain the title compound (2.64 g).

Provenance & Evidence