HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol hydrochloride → HCID 66884092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol hydrochloride | HCID 21887872 | — |
| Reactant | HCID 43348316 | HCID 43348316 | — |
| Reactant | HCID 66884093 | HCID 66884093 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66884092 | HCID 66884092 | — |
Reaction Steps
By a similar method as in Example 1, 1-[5-(4-benzo[b]thiophen-4-yl-piperazin-1-yl)pentyl]-3,4-dihydro-1H-quinolin-2-one was prepared from 1-(5-chloropentyl)-3,4-dihydro-1H-quinolin-2-one, and after it was made into an ethanol solution, 1N hydrochloric acid ethanol solution was added thereto, precipitated crystals were separated by filtration and thereby 1-[5-(4-benzo[b]thiophen-4-yl-piperazin-1-yl)pentyl]-3,4-dihydro-1H-quinolin-2-one hydrochloride was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206167B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-9406a2c6869d47da9ff30968abca3f6b |
| Source note | uspto-grants-2015_12 |