Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 67327927 | HCID 67327927 | — |
| Product | HCID 178516493 | HCID 178516493 | 100% |
Reaction Steps
48% Aqueous hydrogen bromide (19.50 mL) was added to 3-(4-methoxypyrimidin-2-yl) pyrazolo[1,5-a]pyridine (Preparation 4a, 0.30 g, 1.32 mmol) and the resulting mixture was heated to 100° C. with stirring. After 3 hours, the mixture was cooled and the resultant precipitate was filtered and dried in vacuo to give the title compound (0.28 g, 99%) as the hydrobromide salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09206183B2 |
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| Source dataset | uspto-grants-2015_12 |
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| ORD ID | ord-625c7ff4699a489280a8c607c82d84bc |
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| Source note | uspto-grants-2015_12 |
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