HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)pyrazolo[1,5-a]pyridine → 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-YL)pyrazolo(1, 5-A)pyrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)pyrazolo[1,5-a]pyridine | HCID 58385948 | — |
| Reactant | 3-Bromopyrazolo[1,5-a]pyrazine | HCID 67123766 | — |
| Product | 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-YL)pyrazolo(1, 5-A)pyrazine | HCID 67372227 | — |
Reaction Steps
Obtained from 3-bromopyrazolo[1,5-a]pyrazine (Preparation 23c) following the experimental procedure as described in Preparation 27a, irradiating the reaction mixture at 100° C. for 1 h. The crude product was used without further purification in the next synthetic step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206183B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-08a8de0563c54274995f2ad38eeb4d52 |
| Source note | uspto-grants-2015_12 |