HRID1501234

反应详情

EQUATION

反应方程式

HRID 1501234 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of tert-butyl 2-methyl-4-(1-phenylethyl)benzoate (1.6 g, 5.4 mmol) in dichloromethane 9 mL, and 3 mL trifluoroacetic acid was added. The mixture was stirred 0.5 hour. Thin layer chromatography showed full conversion. The reaction mixture was concentrated to give 2-methyl-4-(1-phenylethyl)benzoic acid (1 g, 90%).

WORKUP

后处理

  1. concentrationThe reaction mixture was concentrated