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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1501279Generated: October 27, 2026

Phenethyl bromide → HCID 131734281, compound

https://huagongshe.com/reaction/1501279

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenethyl bromideHCID 7666—
ReactantEthyl 3,5-dimethylisonicotinateHCID 59589494—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 131734281HCID 131734281—

Reaction Steps

1-(bromoethyl)benzene (1.3 g, 7.03 mmol) was added to ethyl 3,5-dimethylisonicotinate (0.7 g, 3.91 mmol) in dioxane (20 mL) and the resultant mixture was stirred at reflux overnight. The resulting solution was used to the next step without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09206128B2
Source datasetuspto-grants-2015_12
ORD IDord-1545a96e18274b38a21c98eaddbfa007
Source noteuspto-grants-2015_12