HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethyl bromide → HCID 131734281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | Ethyl 3,5-dimethylisonicotinate | HCID 59589494 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 131734281 | HCID 131734281 | — |
Reaction Steps
1-(bromoethyl)benzene (1.3 g, 7.03 mmol) was added to ethyl 3,5-dimethylisonicotinate (0.7 g, 3.91 mmol) in dioxane (20 mL) and the resultant mixture was stirred at reflux overnight. The resulting solution was used to the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206128B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-1545a96e18274b38a21c98eaddbfa007 |
| Source note | uspto-grants-2015_12 |