HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxygen → Tcep mpaa
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxygen | HCID 977 | — |
| Reactant | Tris(2-carboxyethyl)phosphine | HCID 119411 | — |
| Reactant | 2-(3-Mercaptophenyl)acetic acid | HCID 3543156 | — |
| Solvent | Phosphate | HCID 1061 | — |
| Product | Tcep mpaa | HCID 131734284 | — |
Reaction Steps
Handling is carried out in a glove box ([O2]<50 ppm). A solution of TCEP at 300 mmol/L is prepared in 0.2 M phosphate buffer at pH=7.2. 3-Mercaptophenylacetic acid (MPAA) (84 mg, 0.5 mmol) is then added. The pH of the TCEP/MPAA solution obtained is adjusted to pH=6.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206224B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-32d60538298644b4ae8105da88788056 |
| Source note | uspto-grants-2015_12 |