HRID1502169
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
6-(1H-Tetrazol-1-yl)pyridin-3-amine (50 mg, 0.308 mmol) was dissolved in pyridine (1.5 mL), followed by addition of phenyl chloroformate (53.1 mg, 0.339 mmol). The mixture was stirred at RT overnight, and was concentrated to give crude title compound. LC/MS: [(M+1]+=283.14, [(M+1-28)]+=255.13.
WORKUP
后处理
- concentrationwas concentrated