HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl chloroformate → phenyl[6-(1H-tetrazol-1-yl)pyridin-3-yl]carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | 6-(1H-1,2,3,4-tetrazol-1-yl)pyridin-3-amine | HCID 66927338 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | phenyl[6-(1H-tetrazol-1-yl)pyridin-3-yl]carbamate | HCID 117693882 | — |
Reaction Steps
6-(1H-Tetrazol-1-yl)pyridin-3-amine (50 mg, 0.308 mmol) was dissolved in pyridine (1.5 mL), followed by addition of phenyl chloroformate (53.1 mg, 0.339 mmol). The mixture was stirred at RT overnight, and was concentrated to give crude title compound. LC/MS: [(M+1]+=283.14, [(M+1-28)]+=255.13.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206199B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-d7d74cbc5d9748959ebd48eaa2c052e5 |
| Source note | uspto-grants-2015_12 |