HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 89618840, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 89619100 | HCID 89619100 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 89618840 | HCID 89618840 | — |
Reaction Steps
tert-Butyl 5-(1H-tetrazol-1-yl)pyridin-2-ylcarbamate (300 mg, 1.14 mmol) was dissolved in DCM (2 mL), followed by addition of 4 M HCl in dioxane (2.86 mL, 11.4 mmol). The mixture was stirred at RT for 4 hours, then concentrated to give title compound. LC/MS: [(M+1)]+=163.20.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206199B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-e7bc90844b3f49739f90f0087c0e2b22 |
| Source note | uspto-grants-2015_12 |