Hydrogen Bromide → HCID 11791475, compound

HRID 1502616Notes

Reaction equation

HRID 1502616 reaction equation
Br.[NH2:2][C@H:3]([C:14]([OH:16])=[O:15])[CH2:4][C:5]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[NH:7][CH:6]=1.N1([C:29](=O)[C:28]2N(C)C=N[C:23]=2N(C)C1=O)C>O>[CH:28]([O:15][C:14](=[O:16])[C@H:3]([CH2:4][C:5]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[NH:7][CH:6]=1)[NH2:2])([CH3:29])[CH3:23]

Participants

5

Reactant 3

HCID 260Hydrogen BromideHCID 2519CaffeineHCID 6305L-Tryptophan

Product 1

HCID 11791475HCID 11791475, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

HBr (120 g) and tryptophan (5 g) were dissolved in water (1 L). Caffeine (100 g) was added into the mixture and the mixture was stirred for a few minutes. The mixture was filled into either spray bottles or roll-on bottles.

Workup

  1. additionThe mixture was filled into either spray bottles or roll-on bottles

Sources & evidence

ORD record
ord-0f5bf584fca649009176f05f6dd80157
Source dataset
uspto-grants-2015_12
Patent number
US09211249B2

Reaction notes

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