HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69198469, compound → HCID 71765701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69198469 | HCID 69198469 | — |
| Reactant | HCID 117778387 | HCID 117778387 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 71765701 | HCID 71765701 | 5.5% |
Reaction Steps
N-(4-Cyclohexylphenyl)-6-hydrazinonicotinamide (0.20 g) and 4-(ethoxymethylene)-2-methyl-1,3-oxazol-5(4H)-one (0.12 g) were dissolved in ethanol (30 mL), and the solution was stirred at room temperature for 1.5 hours. The solvent was distilled off under reduced pressure, and diisopropyl ether was added to the residue. The deposited solid was collected by filtration and washed with diisopropyl ether. The solid was dried under reduced pressure to obtain the title compound (0.015 g) as a white solid (yield: 5.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09212170B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-48e4440e87e84b1f9472eb08a16fb575 |
| Source note | uspto-grants-2015_12 |