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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1503236Generated: October 31, 2026

HCID 69198469, compound → HCID 71765701, compound

https://huagongshe.com/reaction/1503236

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69198469HCID 69198469—
ReactantHCID 117778387HCID 117778387—
SolventEthanolHCID 702—
ProductHCID 71765701HCID 717657015.5%

Reaction Steps

N-(4-Cyclohexylphenyl)-6-hydrazinonicotinamide (0.20 g) and 4-(ethoxymethylene)-2-methyl-1,3-oxazol-5(4H)-one (0.12 g) were dissolved in ethanol (30 mL), and the solution was stirred at room temperature for 1.5 hours. The solvent was distilled off under reduced pressure, and diisopropyl ether was added to the residue. The deposited solid was collected by filtration and washed with diisopropyl ether. The solid was dried under reduced pressure to obtain the title compound (0.015 g) as a white solid (yield: 5.5%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09212170B2
Source datasetuspto-grants-2015_12
ORD IDord-48e4440e87e84b1f9472eb08a16fb575
Source noteuspto-grants-2015_12