HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86725376, compound → HCID 69676295, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86725376 | HCID 86725376 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69676295 | HCID 69676295 | — |
Reaction Steps
To a solution of the product of Example 15B (4 g, 8 mmol) in methanol (100 mL) was added 10% palladium on carbon (400 mg). The mixture was stirred at room temperature under hydrogen for 16 hours. The catalyst was filtered off and the filtrate was concentrated to give the title compound. MS: 314 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09212192B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-646f4728bc15410d8a1ad0adfff08e21 |
| Source note | uspto-grants-2015_12 |