HCID 86725407, compound → HCID 86725408, compound

Participants

Reaction Steps

A suspension of the product of Example 51B (2 g, 4.1 mmol) and 10% palladium on carbon (200 mg) in methanol (100 mL) was stirred under hydrogen for 18 hours. The catalyst was filtered and the filtrate was concentrated and the residue was purified by flash chromatography on silica gel (200-300 mesh) eluting with 1/1 petroleum ether/ethyl acetate to give the title compound. MS: 310 (M+H+).

Provenance & Evidence