HuagongsheHuagongshe Chemistry Print Report · For research reference only
zinc(II)iodide → HCID 178506620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | zinc(II)iodide | HCID 9883512 | — |
| Reactant | [(1R,2S,4S)-7-oxabicyclo[2.2.1]heptan-2-yl]methanol | HCID 13614304 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178506620 | HCID 178506620 | — |
Reaction Steps
The title compound was prepared in an analogous manner to tetrahydro-2H-pyran-4-yl)zinc(II) iodide except that (1R,2S,4S)-7-oxabicyclo[2.2.1]heptan-2-ylmethanol was used instead of tetrahydro-2H-pyran-4-ol in Step 1 to afford a 0.15M solution of ((1R,2R,4S)-7-oxabicyclo[2.2.1]heptan-2-ylmethyl)zinc(II) iodide in THF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09212182B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-d8058427b9aa43e1bc21671c5e5022c0 |
| Source note | uspto-grants-2015_12 |