HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4-Difluorocyclohexan-1-ol → HCID 178506004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4-Difluorocyclohexan-1-ol | HCID 546300 | — |
| Reactant | zinc(II)iodide | HCID 9883512 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178506004 | HCID 178506004 | — |
Reaction Steps
The title compound was prepared in an analogous manner to tetrahydro-2H-pyran-4-yl)zinc(II) iodide except that 4,4-difluorocyclohexanol (Affinity Chemicals) was used instead of tetrahydro-2H-pyran-4-ol in Step 1 to afford a 0.26 M solution of (4,4-difluorocyclohexyl)zinc(II) iodide in THF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09212182B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-b276b91074cf43149f567f683956b7d8 |
| Source note | uspto-grants-2015_12 |