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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1504570Generated: October 31, 2026

Triethylamine → HCID 118380271, compound

https://huagongshe.com/reaction/1504570

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantTriphosgeneHCID 94429—
ReactantN-Boc-diethanolamineHCID 4360601—
SolventDichloromethaneHCID 6344—
ProductHCID 118380271HCID 118380271—

Reaction Steps

The procedure of Example 1 was followed using N-boc diethanolamine (3 g, 14.6 mmol), triethylamine (4.1 mL, 29.2 mmol), dry dichloromethane (100 mL) and triphosgene (1.4 g, 4.9 mmol). The filtrate was concentrated yielding only oligomeric compounds.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09215876B2
Source datasetuspto-grants-2015_12
ORD IDord-e881160028974952840763b6267931ac
Source noteuspto-grants-2015_12