HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 118380271, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Reactant | N-Boc-diethanolamine | HCID 4360601 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 118380271 | HCID 118380271 | — |
Reaction Steps
The procedure of Example 1 was followed using N-boc diethanolamine (3 g, 14.6 mmol), triethylamine (4.1 mL, 29.2 mmol), dry dichloromethane (100 mL) and triphosgene (1.4 g, 4.9 mmol). The filtrate was concentrated yielding only oligomeric compounds.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09215876B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-e881160028974952840763b6267931ac |
| Source note | uspto-grants-2015_12 |