HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 131734333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 88447749 | HCID 88447749 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131734333 | HCID 131734333 | — |
Reaction Steps
A solution of EMC-Glu-NH—NH-BOC (32.4 g) and TFA (165 mL) in DCM (165 mL) was stirred at RT for 80 min after which diethyl ether (4 L) was added. The precipitated product was collected by suction filtration, washed with ether and dried yielding EMC-Glu-NH—NH2 TFA (20 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09216228B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-1c6aeaf38b834e2884a0292faebb1e10 |
| Source note | uspto-grants-2015_12 |