HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 56597206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 131734350 | HCID 131734350 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 56597206 | HCID 56597206 | — |
Reaction Steps
The intermediate from Step b) was dissolved in 350 ml of methanol, and 20 drops of a 1 N aqueous sodium hydroxide solution were added (pH=6). The mixture was stirred at RT overnight and concentrated on a rotary evaporator. The residue was purified on silica gel (mobile phase: dichloromethane/methanol, 96:4). This gave 67 mg (15% of theory) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09216978B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-61af5d4802e44e6095d3a75e2f81f400 |
| Source note | uspto-grants-2015_12 |