HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 90404094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 90404884 | HCID 90404884 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 90404094 | HCID 90404094 | — |
Reaction Steps
200 mg of methyl 6-methoxy-5-methyl-1H-indole-2-carboxylate (1 mmol) was heated at 80 degrees in a sealed tube with 2 mL of 7M ammonia in methanol. After one week reaction the solvent evaporated to produce 202 mg of 6-methoxy-5-methyl-1H-indole-2-carboxamide that was used without purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09216993B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-ddbc79c61a294e0686553482aac1ca44 |
| Source note | uspto-grants-2015_12 |