HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59615355, compound → HCID 84663096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59615355 | HCID 59615355 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 84663096 | HCID 84663096 | 102.4% |
Reaction Steps
Methyl 6-nitro-1H-benzimidazole-4-carboxylate (304 mg) was suspended in MeOH (10 mL), the suspension was added with 5% palladium on carbon (30 mg), and stirred under hydrogen (1 atm) atmosphere. The catalyst was filtered off on celite and washed with MeOH, and the mother liquor was concentrated in vacuo to obtain the titled compound (269 mg) as pale yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09216968B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-694f19957d5c4fa699832ad802009e5f |
| Source note | uspto-grants-2015_12 |