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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1505758Generated: October 31, 2026

HCID 59615355, compound → HCID 84663096, compound

https://huagongshe.com/reaction/1505758

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59615355HCID 59615355—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 84663096HCID 84663096102.4%

Reaction Steps

Methyl 6-nitro-1H-benzimidazole-4-carboxylate (304 mg) was suspended in MeOH (10 mL), the suspension was added with 5% palladium on carbon (30 mg), and stirred under hydrogen (1 atm) atmosphere. The catalyst was filtered off on celite and washed with MeOH, and the mother liquor was concentrated in vacuo to obtain the titled compound (269 mg) as pale yellow powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09216968B2
Source datasetuspto-grants-2015_12
ORD IDord-694f19957d5c4fa699832ad802009e5f
Source noteuspto-grants-2015_12