反应详情

3-Bromo-9H-dipyrido[2,3-b;4′,3′-d]pyrrole-6-carboxylic acid methyl ester (140 mg, 0.458 mmol) was dissolved in pyrrolidine (6 mL) and the mixture heated to reflux for 2 h. The mixture was allowed to cool and concentrated in vacuo to afford a bright orange oily solid. The residue was used without purification.

1. temperaturethe mixture heated
2. temperatureto reflux for 2 h
3. temperatureto cool
4. concentrationconcentrated in vacuo
5. customto afford a bright orange oily solid
6. customThe residue was used without purification