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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1506167Generated: October 31, 2026

HCID 136227340, compound → HCID 136341305, compound

https://huagongshe.com/reaction/1506167

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 136227340HCID 136227340—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 136341305HCID 136341305100.1%

Reaction Steps

Benzyl 3-(7H-pyrrolo[3,2-e][1,2,3]triazolo[1,5-c]pyrimidin-1-yl)piperidine-1-carboxylate (25.0 mg, 0.0664 mmol) in ethanol was stirred with 5% palladium-carbon (10 mg) under a hydrogen atmosphere at 50° C. for 2.5 hours. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound as a light brown solid (16.1 mg, yield quantitative).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09216999B2
Source datasetuspto-grants-2015_12
ORD IDord-4c46ba158bb64394bc18a117615939a8
Source noteuspto-grants-2015_12