HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 136341325, compound → HCID 136341327, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 136341325 | HCID 136341325 | — |
| Reactant | HCID 136341328 | HCID 136341328 | — |
| Product | HCID 136341327 | HCID 136341327 | 51% |
Reaction Steps
The reactions in Synthetic Examplea 435 were carried out in substantially the same manners except that ethyl 2-[4-(7H-pyrrolo[3,2-e][1,2,3]triazolo[1,5-c]pyrimidin-1-yl)cyclohexylidene]acetate obtained in Synthetic Examplea 436 was used instead of 2-[4-(7H-pyrrolo[3,2-e][1,2,3]triazolo[1,5-c]pyrimidin-1-yl)cyclohexylidene]acetonitrile to give the title compound as a colorless solid (cis/trans mixture; 29.0 mg, yield 51%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09216999B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-cb7b43be3d7f46b7bb0905b81d6211b3 |
| Source note | uspto-grants-2015_12 |