HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 178496611, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 178496620 | HCID 178496620 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178496611 | HCID 178496611 | 95% |
Reaction Steps
tert-Butyl (trans-4-methoxycyclohexyl)carbamate in ethanol (5 mL) was stirred with acetyl chloride (1.5 mL) for one day under cooling with ice, and the solvent was concentrated under reduced pressure to give the title compound (475 mg, yield 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09216999B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-6fa177b3cd6d47d3a0a132e1b3831867 |
| Source note | uspto-grants-2015_12 |