HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3,4-diethoxybenzoate → 3-(3,4-Diethoxyphenyl)-7-vinyl-4,5-dihydronaphtho[1,2-c]isoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3,4-diethoxybenzoate | HCID 13652158 | — |
| Reactant | 3-(4-Isobutyl-3-(trifluoromethyl)phenyl)-7-vinyl-4,5-dihydronaphtho[1,2-c]isoxazole | HCID 67169184 | — |
| Reactant | 6-vinyl-3,4-dihydronaphthalen-1(2H)-one oxime | HCID 86669866 | — |
| Product | 3-(3,4-Diethoxyphenyl)-7-vinyl-4,5-dihydronaphtho[1,2-c]isoxazole | HCID 67170297 | — |
Reaction Steps
This compound was prepared according to the general procedure described for Preparation 23C, employing 200 mgs of 6-vinyl-3,4-dihydronaphthalen-1(2H)-one oxime (I-1) and methyl 3,4-diethoxybenzoate (1 eq). Yield: 217 mgs (25%); LC/MS M+1=362.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09216972B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-63477ac5175c40a48a03595f9887ce66 |
| Source note | uspto-grants-2015_12 |