HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3,4-Diethoxyphenyl)-7-vinyl-4,5-dihydronaphtho[1,2-c]isoxazole → 3-(3,4-Diethoxyphenyl)-4,5-dihydronaphtho[1,2-c]isoxazole-7-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3,4-Diethoxyphenyl)-7-vinyl-4,5-dihydronaphtho[1,2-c]isoxazole | HCID 67170297 | — |
| Reactant | 3-(4-Isobutyl-3-(trifluoromethyl)phenyl)-4,5-dihydronaphtho[1,2-c]isoxazole-7-carbaldehyde | HCID 86669886 | — |
| Product | 3-(3,4-Diethoxyphenyl)-4,5-dihydronaphtho[1,2-c]isoxazole-7-carbaldehyde | HCID 86669921 | — |
Reaction Steps
This compound was prepared according to the general procedure described for Preparation 23D, employing 67 mgs of 3-(3,4-diethoxyphenyl)-7-vinyl-4,5-dihydronaphtho[1,2-c]isoxazole (80A). Yield: 67 mgs (99%); LC/MS M+1=364.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09216972B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-995df1017d814175a7a82f9d9f7cb796 |
| Source note | uspto-grants-2015_12 |