HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(6-bromo-1-oxo-1,2,3,4-tetrahydronaphthalen-2-yl)hexanamide → 7-Bromo-2-pentyl-4,5-dihydronaphtho[2,1-d]thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(6-bromo-1-oxo-1,2,3,4-tetrahydronaphthalen-2-yl)hexanamide | HCID 67168280 | — |
| Reactant | 5-(7-Bromo-4,5-dihydronaphtho[2,1-d]thiazol-2-yl)-3-phenyl-4-(trifluoromethyl)isoxazole | HCID 67171464 | — |
| Product | 7-Bromo-2-pentyl-4,5-dihydronaphtho[2,1-d]thiazole | HCID 68182078 | — |
Reaction Steps
This compound was prepared according to the procedure described for Preparation 82D, employing 1.25 g of N-(6-bromo-1-oxo-1,2,3,4-tetrahydronaphthalen-2-yl)hexanamide (86A). Yield: (415 mgs, 33%). LC/MS M+1=337.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09216972B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-94f82244044a43289986d1912ae49821 |
| Source note | uspto-grants-2015_12 |