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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1506532Generated: October 30, 2026

6-iodo-3,4-dihydronaphthalen-1(2H)-one → (NE)-N-(6-iodo-3,4-dihydro-2H-naphthalen-1-ylidene)hydroxylamine

https://huagongshe.com/reaction/1506532

Reaction equation

Participants

RoleNameHCIDCharge
Reactant6-iodo-3,4-dihydronaphthalen-1(2H)-oneHCID 45489800—
Reactant(NE)-N-(5-ethenyl-2,3-dihydroinden-1-ylidene)hydroxylamineHCID 87295219—
Product(NE)-N-(6-iodo-3,4-dihydro-2H-naphthalen-1-ylidene)hydroxylamineHCID 140592659—

Reaction Steps

The titled compound was prepared using the experimental protocol described for Preparation 87B employing 6-iodo-3,4-dihydronaphthalen-1(2H)-one as a starting material. The compound had an HPLC retention time=3.28 min. (condition C); LC/MS M+1=288.1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09216972B2
Source datasetuspto-grants-2015_12
ORD IDord-408dcd7e99594248bd95bfb735ffff00
Source noteuspto-grants-2015_12