HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(1-phenyl-5-(trifluoromethyl)-1H-pyrazol-4-yl)-7-vinyl-4,5-dihydronaphtho[1,2-c]isoxazole → HCID 67171291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(1-phenyl-5-(trifluoromethyl)-1H-pyrazol-4-yl)-7-vinyl-4,5-dihydronaphtho[1,2-c]isoxazole | HCID 67170420 | — |
| Reactant | ethyl 1-(5-fluoropyridin-2-yl)-5-(trifluoromethyl)-1H-pyrazole-4-carboxylate | HCID 67171373 | — |
| Reactant | 6-vinyl-3,4-dihydronaphthalen-1(2H)-one oxime | HCID 86669866 | — |
| Product | HCID 67171291 | HCID 67171291 | — |
Reaction Steps
The titled compound was prepared using the experimental protocol described for Preparation 89A employing 6-vinyl-3,4-dihydronaphthalen-1(2H)-one oxime (I-1) and ethyl 1-(5-fluoropyridin-2-yl)-5-(trifluoromethyl)-1H-pyrazole-4-carboxylate (Preparation 122A) as starting materials. The compound had an HPLC retention time=3.93 min. (condition C); LC/MS M+1=426.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09216972B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-fb6490b76b7e416eabe0ff43714b7fde |
| Source note | uspto-grants-2015_12 |