huagongshe.com
HRID1506629

反应详情

EQUATION

反应方程式

HRID 1506629 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)NN
HCID14039

Monoacetyl hydrazine

C2H6N2O

结构：CCOC(=O)C(Cl)=Nc1ccccc1C
HCID90280270

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1nnc(C)n1-c1ccccc1C
HCID90281310

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

The suspension of 10B and acetohydrazide in acetonitrile was refluxed for 2 hours. The solvent was removed. The crude product was purified by flash column (Rf: 0.2, 50% EtOAc/Hexanes). MS (m/z) 246 [M+H]+.

WORKUP

后处理

  1. temperaturewas refluxed for 2 hours
  2. customThe solvent was removed
  3. customThe crude product was purified by flash column (Rf: 0.2, 50% EtOAc/Hexanes)