HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70982893, compound → 4-(Pyrrolidin-1-yl)butan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70982893 | HCID 70982893 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 4-(Pyrrolidin-1-yl)butan-1-amine | HCID 2762762 | 82.2% |
Reaction Steps
To a solution of benzyl 4-(pyrrolidin-1-yl)butylcarbamate (196 mg, 0.71 mmol) was added catalytic amount of Pd/C (5%). The reaction was stirred under a hydrogen atmosphere overnight and filtered. The filtrate was concentrated to give 4-(pyrrolidin-1-yl)butan-1-amine (83 mg)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221760B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-4bdf11b76ca04cc290690068dd55cd3a |
| Source note | uspto-grants-2015_12 |