Ethylamine → HCID 70982982, compound

HRID 1506755Notes

Reaction equation

HRID 1506755 reaction equation
CS(O[CH2:6][CH2:7][CH2:8][CH2:9][NH:10][C:11]([O:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[O:12])(=O)=O.[CH2:21]([NH2:23])[CH3:22]>C1COCC1>[CH2:21]([NH:23][CH2:6][CH2:7][CH2:8][CH2:9][NH:10][C:11](=[O:12])[O:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)[CH3:22]

Participants

4

Reactant 2

HCID 6341EthylamineHCID 11141145N-(benzyloxycarbonyl)-4-(mesyloxy)butylamine

Product 1

HCID 70982982HCID 70982982, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Following the general procedure of Example 4, Step 2, and making non-critical variations but using 4-(benzyloxycarbonylamino)butyl methanesulfonate and ethyl amine in THF, the compound of Step 1 was obtained.

Sources & evidence

ORD record
ord-4457af918cd942f392648480225a7911
Source dataset
uspto-grants-2015_12
Patent number
US09221760B2

Reaction notes

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