Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 70983743 | HCID 70983743 | — |
| Product | HCID 86720060 | HCID 86720060 | — |
Reaction Steps
The mixture of benzyl 4-(cyclopropyl(ethyl)amino)butylcarbamate (Step 1) in HCl (6 N) was heated to reflux for 1 hour and cooled to 20-25° C. The reaction mixture was concentrated, and the residue was dried under reduced pressure to give N1-cyclopropyl-N1-ethylbutane-1,4-diamine HCl salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09221760B2 |
|---|
| Source dataset | uspto-grants-2015_12 |
|---|
| ORD ID | ord-f112d18139d249e2944abb7e67a4c7bd |
|---|
| Source note | uspto-grants-2015_12 |
|---|
