HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoic Acid → HCID 71656517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoic Acid | HCID 6318 | — |
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | N-(2-Butyl-1-benzofuran-5-yl)methanesulfonamide | HCID 9878493 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 71656517 | HCID 71656517 | — |
Reaction Steps
4.02 g of 4-chlorobenzoyl chloride—prepared by reacting 4-chlorobenzoic acid with thionyl chloride—and 5.42 g of 2-butyl-5-methanesulfonamido-benzofuran (IV) were dissolved in 30 ml of dichloromethane. The reaction was performed according to Example 10.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221777B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-55574ad9fca343b5ad1bda5bbe199ef6 |
| Source note | uspto-grants-2015_12 |