Hydrochloric Acid → HCID 13758018, compound

HRID 1506859Notes

Reaction equation

HRID 1506859 reaction equation
[F:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[CH:11]([CH3:15])[C:12]([OH:14])=[O:13].Cl.[CH3:17]O>>[F:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[CH:11]([CH3:15])[C:12]([O:14][CH3:17])=[O:13]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 13758016HCID 13758016, compound

Product 1

HCID 13758018HCID 13758018, compoundYield 93%

Procedure

Compound (5) obtained above was esterified by adding a catalytic amount of concentrated hydrochloric acid in methanol to give compound (6) of interest as a clear yellow oil at a yield of 93%.

Sources & evidence

ORD record
ord-b7ecfe7d3da44073b4f46eef6c70923f
Source dataset
uspto-grants-2015_12
Patent number
US09221786B2

Reaction notes

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