HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 60155536, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 60155535 | HCID 60155535 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 60155536 | HCID 60155536 | 82.3% |
Reaction Steps
A solution of compound (26a) (10.8 g, 32.6 mmol) in acetic acid (36 mL), and concentrated sulfuric acid (10 mL), and water (26 mL) were treated in the same manner as in (b) in Production Example 1 to give 6.2 g (82%) of compound (27a) as yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221786B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-1adc797fed2e4e178ee24037cb52a4af |
| Source note | uspto-grants-2015_12 |