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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1506880Generated: October 30, 2026

Methanol → HCID 60155537, compound

https://huagongshe.com/reaction/1506880

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 60155536HCID 60155536—
SolventHydrochloric AcidHCID 313—
ProductHCID 60155537HCID 6015553790%

Reaction Steps

Compound (27a) (6.2 g, 26.8 mmol) was dissolved in a solution of a catalytic amount of concentrated hydrochloric acid (0.24 mL) in methanol (123 mL) and treated in the same manner as in (c) in Production Example 1 to give 5.9 g (90%) of compound (28a) as pale yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09221786B2
Source datasetuspto-grants-2015_12
ORD IDord-b68596fc55e44fafbd6300a68e23fc99
Source noteuspto-grants-2015_12