HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 60155537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 60155536 | HCID 60155536 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 60155537 | HCID 60155537 | 90% |
Reaction Steps
Compound (27a) (6.2 g, 26.8 mmol) was dissolved in a solution of a catalytic amount of concentrated hydrochloric acid (0.24 mL) in methanol (123 mL) and treated in the same manner as in (c) in Production Example 1 to give 5.9 g (90%) of compound (28a) as pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221786B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-b68596fc55e44fafbd6300a68e23fc99 |
| Source note | uspto-grants-2015_12 |