HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 117676157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2-(2,6-Difluoro-4-nitrophenyl)propanoic acid | HCID 53429568 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 117676157 | HCID 117676157 | 89% |
Reaction Steps
Compound (27b) (3.6 g, 15.6 mmol) was dissolved in a solution of a catalytic amount of concentrated hydrochloric acid (0.14 mL) in methanol (72 mL) and treated in the same manner as in (c) in Production Example 1 to give 3.4 g (89%) of compound (28b) as pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221786B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-4f507540534e416d9131d48014a96221 |
| Source note | uspto-grants-2015_12 |