HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 123538816, compound → HCID 123785902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 123538816 | HCID 123538816 | — |
| Reactant | HCID 123891295 | HCID 123891295 | — |
| Product | HCID 123785902 | HCID 123785902 | 70% |
Reaction Steps
The substantially same method as described in Example 351 was conducted, except that (1S,2S)-4-(tert-butyldimethylsilyloxy)-1-(2-chlorophenyl)butane-1,2-diol (Preparation example 353) was used instead of 1R, 2R)-4-(tert-butyldimethylsilyloxy)-1-(2-chlorophenyl)butane-1,2-diol (Preparation example 349), to obtain the title compound (0.7 g, 70˜95%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221783B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-bc828c64523b4f679157506d111f26c4 |
| Source note | uspto-grants-2015_12 |