Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Nitroresorcinol | HCID 11760 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Aminoresorcinol | HCID 69451 | 75% |
Reaction Steps
To a solution of 2-nitrobenzene-1,3-diol (5.00 g, 32.2 mmol) in MeOH (100 mL) was added Pd/C (200 mg). The mixture was stirred under a H2 atmosphere at 25° C. for 16 h, filtered, and concentrated. The crude product was used in the next step without further purification. (3.00 g, yield 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09221794B2 |
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| Source dataset | uspto-grants-2015_12 |
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| ORD ID | ord-f086a722ae02452aad5ae4954f8f19f4 |
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| Source note | uspto-grants-2015_12 |
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