HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Amino-1-butanol → HCID 90375154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Amino-1-butanol | HCID 25868 | — |
| Reactant | Ethyl 2-formylpyridine-4-carboxylate | HCID 19600808 | — |
| Product | HCID 90375154 | HCID 90375154 | — |
Reaction Steps
By General Procedure A from ethyl 2-formylpyridine-4-carboxylate and 4-aminobutan-1-ol. Purification by column chromatography (5% MeOH/DCM) gave the target compound as greenish oil. 1H-NMR (300 MHz, CDCl3): δ 8.60 (d, 1H), 7.80 (s, 1H), 7.70 (d, 1H), 4.40 (q, 2H), 4.05 (s, 1H), 3.60 (m, 2H), 2.80 (m, 2H), 1.70 (m, 4H), 1.40 (t, 3H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221801B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-96edbbb67de14f239d0427044eb62d5e |
| Source note | uspto-grants-2015_12 |