HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzaldehyde → HCID 90094314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Reactant | HCID 90093924 | HCID 90093924 | — |
| Product | HCID 90094314 | HCID 90094314 | — |
Reaction Steps
Prepared by General Procedure A from 2-methoxybenzaldehyde and ethyl 2-[(2,2,2-trifluoro-N-{[(piperidin-4-yl)carbamoyl]methyl}acetamido)methyl]pyridine-4-carboxylate. 1H-NMR (300 MHz, CDCl3): δ 8.75 & 8.71 (2d, 1H; rotamer), 7.91-7.78 (m, 2H), 7.36 (m, 1H), 7.25 (m, 1H), 7.99-7.86 (m, 2H), 4.95 & 4.72 (2s, 2H, rotamer), 4.45 (q, 2H), 4.30 & 4.08 (2s, 2H; rotamer), 3.83 (m, 4H), 3.60 (m, 2H) 2.95 (m, 2H), 2.22 (m, 2H), 1.90 (m, 2H), 1.60 (m, 2H), 1.40 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221801B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-bb3b65c3cf1b4a97befbebbe9467af63 |
| Source note | uspto-grants-2015_12 |